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     data   graph     files  public [XRD data and results for OAE North Atlantic experiments] - X-ray diffraction (XRD) raw data
and Rietveld refinement results for precipitates from shipboard ocean alkalinity
enhancement (OAE) experiments in the North Atlantic on R/V Atlantic Explorer cruise AE2320 in
September 2023 (OCE-PRF: Towards Quantifying Calcium Carbonate Sediment Dissolution During
Marine Diagenesis)
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The Dataset's Variables and Attributes

Row Type Variable Name Attribute Name Data Type Value
attribute NC_GLOBAL cdm_data_type String Other
attribute NC_GLOBAL Conventions String COARDS, CF-1.6, ACDD-1.3
attribute NC_GLOBAL creator_email String info at bco-dmo.org
attribute NC_GLOBAL creator_name String BCO-DMO
attribute NC_GLOBAL creator_url String https://www.bco-dmo.org/ (external link)
attribute NC_GLOBAL doi String 10.26008/1912/bco-dmo.963717.1
attribute NC_GLOBAL infoUrl String https://osprey.bco-dmo.org/dataset/963717 (external link)
attribute NC_GLOBAL institution String BCO-DMO
attribute NC_GLOBAL license String The data may be used and redistributed for free but is not intended
for legal use, since it may contain inaccuracies. Neither the data
Contributor, ERD, NOAA, nor the United States Government, nor any
of their employees or contractors, makes any warranty, express or
implied, including warranties of merchantability and fitness for a
particular purpose, or assumes any legal liability for the accuracy,
completeness, or usefulness, of this information.
attribute NC_GLOBAL sourceUrl String (local files)
attribute NC_GLOBAL summary String To explore mineral formation due to alkalinity addition, we present results from shipboard experiments in which an aqueous solution of NaOH was added to unfiltered seawater collected from the surface ocean in the Sargasso Sea. Alkalinity addition ranged from 500 to 2000 micromoles per kilogram (µmol/kg) and the carbonate chemistry was monitored through time by measuring total alkalinity (TA) and dissolved inorganic carbon (DIC), which were used to calculate Ω. The amount of precipitate and its minerology were determined throughout the experiments. Mineral precipitation took place in all experiments over a timescale of hours to days. The dominant mineralogy of precipitate is aragonite with trace amounts of calcite and brucite. Aragonite crystallite size increases and its micro-strain decreases with time, consistent with Ostwald ripening. This dataset contains raw XRD data as well as XRD results (mineral abundances, crystallite size, strain, and unit cell parameters) determined via Rietveld refinement. The seawater for the experiments was collected near the Bermuda Atlantic Time Series (31.6667 N, 64.1667 W), which is also the same location where the experiments were conducted and filtered to obtain the precipitates, which were analyzed with XRD.
attribute NC_GLOBAL title String [XRD data and results for OAE North Atlantic experiments] - X-ray diffraction (XRD) raw data and Rietveld refinement results for precipitates from shipboard ocean alkalinity enhancement (OAE) experiments in the North Atlantic on R/V Atlantic Explorer cruise AE2320 in September 2023 (OCE-PRF: Towards Quantifying Calcium Carbonate Sediment Dissolution During Marine Diagenesis)
variable Experiment_name   String  
attribute Experiment_name long_name String Experiment_name
attribute Experiment_name units String unitless
variable Alkalinity_addition   int  
attribute Alkalinity_addition actual_range int 500, 2000
attribute Alkalinity_addition long_name String Alkalinity_addition
attribute Alkalinity_addition units String micromoles per kilogram (umol/kg)
variable Sample   String  
attribute Sample long_name String Sample
attribute Sample units String unitless
variable Exp_start_day   String  
attribute Exp_start_day long_name String Exp_start_day
attribute Exp_start_day units String unitless
variable Exp_start_time   String  
attribute Exp_start_time long_name String Exp_start_time
attribute Exp_start_time units String unitless
variable Filtration_start_day   String  
attribute Filtration_start_day long_name String Filtration_start_day
attribute Filtration_start_day units String unitless
variable Filtration_time   String  
attribute Filtration_time long_name String Filtration_time
attribute Filtration_time units String unitless
variable Filtration_end_day   String  
attribute Filtration_end_day long_name String Filtration_end_day
attribute Filtration_end_day units String unitless
variable Filtration_end_time   String  
attribute Filtration_end_time long_name String Filtration_end_time
attribute Filtration_end_time units String unitless
variable Duration_till_filtration_started   float  
attribute Duration_till_filtration_started actual_range float 0.25, 122.92
attribute Duration_till_filtration_started long_name String Duration_till_filtration_started
attribute Duration_till_filtration_started units String hours
variable Duration_till_filtration_ended   float  
attribute Duration_till_filtration_ended actual_range float 0.92, 125.5
attribute Duration_till_filtration_ended long_name String Duration_till_filtration_ended
attribute Duration_till_filtration_ended units String hours
variable Experiment_mean_duration   float  
attribute Experiment_mean_duration actual_range float 0.58, 124.21
attribute Experiment_mean_duration long_name String Experiment_mean_duration
attribute Experiment_mean_duration units String hours
variable Filtration_duration   float  
attribute Filtration_duration actual_range float 0.23, 2.58
attribute Filtration_duration long_name String Filtration_duration
attribute Filtration_duration units String hours
variable Aragonite   float  
attribute Aragonite actual_range float 35.5, 97.27
attribute Aragonite long_name String Aragonite
attribute Aragonite units String percent
variable Calcite   float  
attribute Calcite actual_range float 0.08, 1.9
attribute Calcite long_name String Calcite
attribute Calcite units String percent
variable Halite   float  
attribute Halite actual_range float 2.25, 62.6
attribute Halite long_name String Halite
attribute Halite units String percent
variable Total   float  
attribute Total actual_range float 99.9, 100.0
attribute Total long_name String Total
attribute Total units String percent
variable Aragonite_and_calcite_total   float  
attribute Aragonite_and_calcite_total actual_range float 37.4, 97.75
attribute Aragonite_and_calcite_total long_name String Aragonite_and_calcite_total
attribute Aragonite_and_calcite_total units String percent
variable Normalized_aragonite   float  
attribute Normalized_aragonite actual_range float 94.92, 99.92
attribute Normalized_aragonite long_name String Normalized_aragonite
attribute Normalized_aragonite units String percent
variable Normalized_calcite   float  
attribute Normalized_calcite actual_range float 0.08, 2.0
attribute Normalized_calcite long_name String Normalized_calcite
attribute Normalized_calcite units String percent
variable Aragonite_crystallite_size_L   int  
attribute Aragonite_crystallite_size_L actual_range int 61, 126
attribute Aragonite_crystallite_size_L long_name String Aragonite_crystallite_size_l
attribute Aragonite_crystallite_size_L units String nanometers (nm)
variable Crystallite_size_error   int  
attribute Crystallite_size_error actual_range int 1, 4
attribute Crystallite_size_error long_name String Crystallite_size_error
attribute Crystallite_size_error units String nanometers (nm)
variable aragonite_strain_L   float  
attribute aragonite_strain_L actual_range float 0.019, 0.099
attribute aragonite_strain_L long_name String Aragonite_strain_l
attribute aragonite_strain_L units String percent
variable strain_error   float  
attribute strain_error actual_range float 1.0E-4, 0.0089
attribute strain_error long_name String Strain_error
attribute strain_error units String percent
variable Aragonite_unit_cell_a   float  
attribute Aragonite_unit_cell_a actual_range float 4.96265, 4.96603
attribute Aragonite_unit_cell_a long_name String Aragonite_unit_cell_a
attribute Aragonite_unit_cell_a units String angstroms
variable Aragonite_unit_cell_b   float  
attribute Aragonite_unit_cell_b actual_range float 7.96702, 7.97512
attribute Aragonite_unit_cell_b long_name String Aragonite_unit_cell_b
attribute Aragonite_unit_cell_b units String angstroms
variable Aragonite_unit_cell_c   float  
attribute Aragonite_unit_cell_c actual_range float 5.75017, 5.75333
attribute Aragonite_unit_cell_c long_name String Aragonite_unit_cell_c
attribute Aragonite_unit_cell_c units String angstroms

The information in the table above is also available in other file formats (.csv, .htmlTable, .itx, .json, .jsonlCSV1, .jsonlCSV, .jsonlKVP, .mat, .nc, .nccsv, .tsv, .xhtml) via a RESTful web service.


 
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